HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → 3-Amino-2-cyano-3-isopropoxy-2-propenenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | Potassium Tricyanomethanide | HCID 10964525 | — |
| Product | 3-Amino-2-cyano-3-isopropoxy-2-propenenitrile | HCID 21396806 | — |
Reaction Steps
In the manner of Example V A, 129.2 g of potassium tricyanomethanide and 1000 ml of isopropanol were treated with 65 ml (96 g) of methanesulfonic acid to yield 104 g of 3-amino-2-cyano-3-isopropoxy-2-propenenitrile, which was used as an intermediate without further purification. The ir spectrum was consistent with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04059433 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-ebcaab2312b84e17a3ab42eb93a35b89 |
| Source note | uspto-grants-1977_11 |