HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylaniline → N-Methylacetanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | Dipropan-2-yl hydrogen phosphite | HCID 558181 | — |
| Product | N-Methylacetanilide | HCID 11364 | 53% |
Reaction Steps
Example 34 was repeated, except that 0.05 mole of phosphorous diisopropyl ester was used in place of phosphorous monoethyl ester and 0.05 mole of N-methylaniline was used in place of aniline, to obtain N-methylacetanilide, yield 53% based on N-methylaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04059603 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-d09be9d3393f48e6a1aaf6ac51f378aa |
| Source note | uspto-grants-1977_11 |