HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → N-benzyloxycarbonyl-glycine-phenythio ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Benzyloxycarbonylglycine | HCID 14349 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-benzyloxycarbonyl-glycine-phenythio ester | HCID 22764889 | 69% |
Reaction Steps
Using thiophenol and Z-Gly.OH, Example 78 was repeated, except that dichloromethane was used in place of ethyl acetate as the extraction solvent, to obtain N-benzyloxycarbonyl glycine phenylthio ester (hereinafter represented by ##STR12## in a yield of 69%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04059603 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-1c401c24185942fc92e919444058368a |
| Source note | uspto-grants-1977_11 |