Thionyl Chloride → HCID 21397987, compound

HRID 1439469Notes

Reaction equation

HRID 1439469 reaction equation
O[CH:2]([CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[CH2:3][CH2:4][N:5]1[CH:9]=[CH:8][N:7]=[CH:6]1.S(Cl)([Cl:17])=O>>[ClH:17].[Cl:17][CH:2]([CH2:10][CH2:11][CH2:12][CH2:13][CH3:14])[CH2:3][CH2:4][N:5]1[CH:9]=[CH:8][N:7]=[CH:6]1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 20282535HCID 20282535, compound

Product 1

HCID 21397987HCID 21397987, compound

Procedure

A solution of 1.5 g of 1-(3-hydroxyoctyl)imidazole was treated with 5 ml. of thionyl chloride and the solution stirred at room temperature for one hour. Evaporation to dryness afforded 1-(3-chlorooctyl)imidazole hydrochloride.

Workup

  1. customEvaporation to dryness

Sources & evidence

ORD record
ord-19b24f0ffdaa47b4b21ba0b2e159c6a8
Source dataset
uspto-grants-1977_11
Patent number
US04059705

Reaction notes

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