HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalic Acid → HCID 20512686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalic Acid | HCID 971 | — |
| Reactant | HCID 20512687 | HCID 20512687 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20512686 | HCID 20512686 | — |
Reaction Steps
A solution of oxalic acid in ether was added dropwise to a stirred solution of 2.0 g. of 1-(3-octylthiooctyl) imidazole in 30 ml. of anhydrous ether until precipitation was complete. The product was filtered off, washed with ether, air dried, and recrystallized from ethyl acetate to yield 1-(3-octylthiooctyl)imidazole oxalate, m.p. 105°-108° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04059705 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-24deb443c54948cba6175b79fde56c01 |
| Source note | uspto-grants-1977_11 |