HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 2-Amino-5-(benzyloxy)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-Amino-5-hydroxybenzamide | HCID 12014920 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Amino-5-(benzyloxy)benzamide | HCID 20338142 | — |
Reaction Steps
A mixture of 5-hydroxyanthranilamide (15.2 g), 250 ml water, 5.1 ml 50% NaOH, and 11.7 ml of benzyl chloride was heated 1/2 at 95°, filtered and the solid recrystallized from 200 ml butanol to give 16.6 g product, m.163-5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060526 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-2b2aea118f3945ec8762248981275d4c |
| Source note | uspto-grants-1977_11 |