反应详情

5-Benzyloxy-2-(2-[4-phenyl-1-piperazinyl]ethylamino)benzamide (1.8 g) in 35 ml ethanol was hydrogenated using 1 g 5% Pd-C catalyst. The mixture was heated to boiling and filtered. The filtrate was cooled and the solid filtered and washed to give 0.7 g product, m.142-3°.

1. temperatureThe mixture was heated
2. filtrationfiltered
3. temperatureThe filtrate was cooled
4. filtrationthe solid filtered
5. washwashed