HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → 1-Iodo-trans-1-octene-3-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | (E)-1-Iodo-1-octen-3-one | HCID 11139597 | — |
| Product | 1-Iodo-trans-1-octene-3-ol | HCID 11043283 | — |
Reaction Steps
Treatment of 63 g. (0.25 mole) of 1-iodo-trans-1-octen3-one (Example 724) with sodium borohydride in the manner described in Example 726 gave 58 g. of yellow oil. The oil is purified by adsorption chromatography on a magnesia silica gel column using benzene as eluent to give a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060540 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-1ca4fb5e49b6493fb2401e71ed9d5969 |
| Source note | uspto-grants-1977_11 |