HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromotriphenylmethane → 1-Bromo-4,4-dimethyl-3-triphenylmethoxy-trans-1-octene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromotriphenylmethane | HCID 11692 | — |
| Reactant | 1-Bromo-4,4-dimethyl-trans-1-octen-3-ol | HCID 20465624 | — |
| Product | 1-Bromo-4,4-dimethyl-3-triphenylmethoxy-trans-1-octene | HCID 20465691 | — |
Reaction Steps
Treatment of 1.88 g. (8 moles) of 1-bromo-4,4-dimethyl-trans-1-octen-3-ol (Example 1174) with 2.58 g. (8 moles) of triphenylmethyl bromide in 20 ml. of pyridine and purification of Florisil ®, all as described in Example 728 gives the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060540 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-ec9965a6f1cd4c4c9b76fe5f816db327 |
| Source note | uspto-grants-1977_11 |