HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22800300, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 22800292 | HCID 22800292 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 22800300 | HCID 22800300 | — |
Reaction Steps
A solution of hydrogen chloride in dioxan (7.5 N, 5 ml) was added to a solution of N-t-butoxycarbonyl-trans-3-methyl-L-prolineamide (0.65 g) in 10 ml dioxan. After 2 hours the crystalline solid was filtered and recrystallised from ethanol/ether to give the product (0.47 g), m.p. 235°-237° [α]D20 -14.8° (c, 1.0, water).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060603 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-fc558da161d64d2dbf68bbf07eedceab |
| Source note | uspto-grants-1977_11 |