HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Glutamic Acid → HCID 178426612, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Glutamic Acid | HCID 33032 | — |
| Reactant | 3,3-Dimethylprolinamide | HCID 20222478 | — |
| Reactant | HCID 178419078 | HCID 178419078 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178426612 | HCID 178426612 | — |
Reaction Steps
This was prepared from 3,3-dimethyl-dl-prolineamide (100 mg) by the method of Example 2(vi) as a white powder (195 mg) m.p. 180° (softening 135°) RF 3B 0.65. Amino acid analysis after acid hydrolysis gave the following ratios: Histidine 1.02, Glutamic acid 0.89 3,3-dimethylproline 1.02 [α]D22 + 5.9° (c = 1, dimethylformamide)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060603 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-92f97a713fc14b06977daff1dc5135c9 |
| Source note | uspto-grants-1977_11 |