HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → N-(4-aminobenzenesulphonyl)iminodithiocarbonic acid dimethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfanilamide | HCID 5333 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Carbon Disulfide | HCID 6348 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Product | N-(4-aminobenzenesulphonyl)iminodithiocarbonic acid dimethyl ester | HCID 86733738 | — |
Reaction Steps
The reaction of 4-aminobenzenesulphonamide (17.2 g) with sodium hydroxide, carbon disulphide and methyl iodide by the method described in Example 8, afforded N-(4-aminobenzenesulphonyl)iminodithiocarbonic acid dimethyl ester (9.4 g), m.p. 202°-204° (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060621 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-9f0378daad8740e28a64b4dfa7ad2b02 |
| Source note | uspto-grants-1977_11 |