2-Bromo-1,3-dimethyl-4-nitrobenzene → 1857357-32-4
Reaction equation
BrC1C(C)=C([N+]([O-])=O)C=CC=1C.[Br:13][C:14]1[C:19]([CH3:20])=[CH:18][CH:17]=[C:16]([N+:21]([O-])=O)[C:15]=1[CH2:24][C:25](=O)[C:26]([OH:28])=[O:27]>>[Br:13][C:14]1[C:19]([CH3:20])=[CH:18][CH:17]=[C:16]2[C:15]=1[CH:24]=[C:25]([C:26]([OH:28])=[O:27])[NH:21]2Participants
3
Procedure
The compound was prepared via 3-bromo-2,4-dimethylnitrobenzene (m.p. 52° C) and 3-(2-bromo-3-methyl-6-nitrophenyl)pyruvic acid (m.p. 196° C).
Sources & evidence
- ORD record
- ord-128cb6f2c9e0498bae312748c286ec44
- Source dataset
- uspto-grants-1977_11
- Patent number
- US04060626
Reaction notes
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