HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl isothiocyanate → HCID 13023177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl isothiocyanate | HCID 128851 | — |
| Reactant | 4-Amino-3-(3'-methoxycarbonyl-2'-thioureido)benzophenone | HCID 3036972 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 13023177 | HCID 13023177 | 54% |
Reaction Steps
To a suspension of 3-(3-carbomethoxythioureido)-4-aminobenzophenone (1.2 g.; 0.0036 mole) in acetone (15 ml.) is added acetyl isothiocyanate (0.37 g.; 0.0036 mole). The reaction mixture is heated to reflux and then allowed to stand at room temperature for 18 hours. The product is collected by filtration, washed successively to afford 0.85 g. (54% yield) of 3-(3-carbomethoxythioureido)-4-(3-acetylthioureido)benzophenone, m.p. 210° C., dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060636 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-f4bd53ad8f0e437d9f29edfe8a006ed8 |
| Source note | uspto-grants-1977_11 |