HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 13023186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 4-Amino-3-(3'-methoxycarbonyl-2'-thioureido)benzophenone | HCID 3036972 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 13023186 | HCID 13023186 | 65% |
Reaction Steps
To a suspension of 3-(3-carbomethoxythioureido)-4-aminobenzophenone (3.29 g.) in toluene (200 ml.) is added benzoyl chloride (1.4 g.). The mixture is refluxed for 18 hours, cooled to room temperature and the precipitate collected, washed with hexane and dried to afford 2.8 g. (65% yield) of 3-(3-carbomethoxythioureido)-4-benzamidobenzophenone as a gray solid, m.p. 191°-192° C., dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060636 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-34cae001ec5e40cd9d5211ae9821a60a |
| Source note | uspto-grants-1977_11 |