Thionyl Chloride → HCID 20130038, compound

HRID 1439985Notes

Reaction equation

[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6](=[CH2:10])[C:7](O)=[O:8].S(Cl)([Cl:13])=O>>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6](=[CH2:10])[C:7]([Cl:13])=[O:8]

Participants

Reactant 2

HCID 24386Thionyl Chloride2×

HCID 3162592-(Furan-2-yl)prop-2-enoic acid

Product 1

HCID 20130038HCID 20130038, compound

Procedure

Furylacrylic acid (marketed by Aldrich) and excess thionyl chloride, SOCl2, are first reacted together at reflux for several hours in order to obtain furylacrylic acid chloride.

Workup

temperatureat reflux for several hours in order

Sources & evidence

ORD record: ord-b2f1fedb799242df805310f2381810b4
Source dataset: uspto-grants-1996_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05496899

Reaction notes

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