Methoxymethyl-triphenylphosphonium chloride → HCID 53788522, compound

HRID 1440025Notes

Reaction equation

HRID 1440025 reaction equation
O=[CH:2][CH2:3][CH2:4][CH2:5][C:6]1[CH:18]=[CH:17][C:9]([C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])=[CH:8][CH:7]=1.[Cl-].[CH3:20][O:21][CH2:22][P+](C1C=CC=CC=1)(C1C=CC=CC=1)C1C=CC=CC=1>>[CH3:20][O:21][CH:22]=[CH:2][CH2:3][CH2:4][CH2:5][C:6]1[CH:18]=[CH:17][C:9]([C:10]([O:12][C:13]([CH3:16])([CH3:15])[CH3:14])=[O:11])=[CH:8][CH:7]=1

Participants

3

Reactant 2

HCID 2723798Methoxymethyl-triphenylphosphonium chlorideHCID 10467200HCID 10467200, compound

Product 1

HCID 53788522HCID 53788522, compound

Procedure

By following the same procedure as described in Reference Example 1, tert-butyl 4-(4-oxobutyl)benzoate (993 mg) was treated with (methoxymethyl)triphenylphosphonium chloride to give the subject compound (918 mg) in the form of a colorless oily substance.

Sources & evidence

ORD record
ord-87bba9d3426d472d9db6542e85349430
Source dataset
uspto-grants-1996_03
Patent number
US05496946

Reaction notes

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