HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 14155016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 2-[(Acetylthio)methyl]-3-phenylpropionic Acid | HCID 9991796 | — |
| Reactant | 29833-32-7 | HCID 12720706 | — |
| Product | HCID 14155016 | HCID 14155016 | — |
Reaction Steps
2-Acetylthiomethyl-3-phenylpropanoic acid is reacted with oxalyl chloride and the resulting acid chloride is then reacted with 11-aminoundecanoic acid, methyl ester, hydrochloride in the presence of diisopropylethylamine as more fully described in Example 12 of European Patent Application 136,883 to give (±)-11-[[2-[(acetylthio)methyl]-1-oxo-3phenylpropyl]amino]undecanoic acid, methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05496805 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-14371b0c49e149eba5428f713f7b6538 |
| Source note | uspto-grants-1996_03 |