HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 18985341, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 1,2-Epoxy-3-fluoropropane | HCID 10418 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18985341 | HCID 18985341 | 100.1% |
Reaction Steps
A solution of 27.28 g (0.359 mole) of epifluorohydrin and 19.20 g (0.1795 mole) of benzylamine dissolved in 200 ml of ethanol was heated under reflux for 4 hours. The reaction mixture was then concentrated by evaporation under reduced pressure, to give 46.6 g of N,N-bis(3-fluoro-2-hydroxypropyl)benzylamine as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05496951 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-d03bc0ca2fe44a0a820d085e55758a10 |
| Source note | uspto-grants-1996_03 |