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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1440177Generated: October 31, 2026

1-Bromopentane → 1-Bromo-4-(pentylsulfanyl)benzene

https://huagongshe.com/reaction/1440177

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-BromopentaneHCID 8057—
ReactantSodium HydroxideHCID 14798—
Reactant4-BromothiophenolHCID 66049—
SolventWaterHCID 962—
Product1-Bromo-4-(pentylsulfanyl)benzeneHCID 12521242—

Reaction Conditions

Temperature90 °C

Reaction Steps

A mixture of 4-bromothiophenol (30 g), pentyl bromide (26.4 g), sodium hydroxide (6.67 g) and water (30 ml) was heated at 90° C. and stirred for 48 hrs. The mixture was then poured into water, extracted with petroleum spirit, dried and distilled (bp 96° C. at 0.11 mmHG). Yield 27.3 g.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05498366
Source datasetuspto-grants-1996_03
ORD IDord-f41c64ede0ed4671b184c0dc50c51544
Source noteuspto-grants-1996_03