HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 178435260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Reactant | HCID 178435390 | HCID 178435390 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Product | HCID 178435260 | HCID 178435260 | 91% |
Reaction Steps
A solution of 4-(2-ethyl-2,3-dihydro-5-nitro-1H-inden-1-yl)-1H-imidazole (10.25 g, 0.03988 mol) in ethanol (150 ml) was hydrogenated over PtO2 (1 g) at 3 atm pressure. When the uptake of hydrogen ceased the reaction mixture was filtered and evaporated to dryness to give 4-(5-amino-2-ethyl-2,3-dihydro-1H-inden-2-yl)-1H-imidazole (8.2 g, 91%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05498623 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-632772bbe19045528e0a9fe708399a1e |
| Source note | uspto-grants-1996_03 |