Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | tert-Butanol | HCID 6386 | — |
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | t-Butyl carbanilate | HCID 137930 | — |
Reaction Steps
Phenylisocyanate (500 g) and tert-butanol (500 mL) are mixed in toluene (500 mL) in a 2 L round bottom flask. The solution is stirred over night in a 50° C. water bath. The N-Boc aniline is collected by filtration to give the white solid (702 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05498624 |
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| Source dataset | uspto-grants-1996_03 |
|---|
| ORD ID | ord-32f4aef637c246e3b91b86b5e11b4d9b |
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| Source note | uspto-grants-1996_03 |
|---|
