HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → 2-Amino-4,6-dimethyl-3-nitropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | Ethene-1,1-diamine, 2-nitro- | HCID 189193 | — |
| Product | 2-Amino-4,6-dimethyl-3-nitropyridine | HCID 298472 | 52% |
Reaction Steps
For the example of the reaction of 1,1-diamino-2-nitroethene with acetylacetone to give 2-amino-3-nitro-4,6-dimethylpyridine, this reaction is described by Troschutz et al., in Arch. Pharm., 325 (1992), 785-789. A yield of 52 percent is described.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05498715 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-1e8e17ed1dfc4d93980c803f4a57c07d |
| Source note | uspto-grants-1996_03 |