HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aminopyridazine → HCID 10087298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aminopyridazine | HCID 230373 | — |
| Reactant | HCID 9991568 | HCID 9991568 | — |
| Reactant | HCID 10087232 | HCID 10087232 | — |
| Product | HCID 10087298 | HCID 10087298 | 24% |
Reaction Steps
5-(Methyl-pyridazin-4-ylmethyl-amino)-8-nitro-naphthalene-1-carbonitrile (24) was prepared in a manner analogous to that described above for the preparation of compound (10), except that compound (9) and pyridazyl amine compound (48) were used as starting materials. Compound (24) (24% yield) was isolated as a yellow foam by flash chromatography on silica, eluting CH2Cl2 :MeOH (25:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05498727 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-bcd7c49f0cd2460188d57c8cc2770130 |
| Source note | uspto-grants-1996_03 |