HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Allylhydroxylamine → HCID 18630364, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Allylhydroxylamine | HCID 420841 | — |
| Reactant | HCID 18630184 | HCID 18630184 | — |
| Product | HCID 18630364 | HCID 18630364 | 86% |
Reaction Steps
The acid prepared in Example 203 was converted to the acid chloride by the procedure of example b. The acid chloride was reacted with aq O-allylhydroxylamine using General Method E1 to afford the title compound. Purification by recrystallization from ether/hexanes gave 0.68 g of the title compound as a white solid in 86% yield. m.p. 92°-94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05498630 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-799f63f390cc4770942900a58d31c5ee |
| Source note | uspto-grants-1996_03 |