HCID 10637720, compound → HCID 10661364, compound

HRID 1440753Notes

Reaction equation

HRID 1440753 reaction equation
[CH3:1][N:2]1[CH2:7][CH2:6][N:5]([CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[Cl:15])[CH2:4][CH:3]1[C:16](OCC)=O.O.Cl.Cl.Cl>>[CH3:1][N:2]1[CH2:7][CH2:6][N:5]([CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[Cl:15])[CH2:4][CH:3]1[C:16]1[NH:2][CH2:3][CH2:4][N:5]=1

Participants

3

Reactant 2

HCID 10637720HCID 10637720, compoundHCID 22037431HCID 22037431, compound

Product 1

HCID 10661364HCID 10661364, compound

Procedure

Yield: 62% (from 1-methyl-4-(2-chlorobenzyl)-2-ethoxycarbonylpiperazine) Melting point: 140°-142° C. (decomposition) (trihydrochloride monohydrate)

Sources & evidence

ORD record
ord-f03831958e394e878b4e46109fe48212
Source dataset
uspto-grants-1996_03
Patent number
US05500426

Reaction notes

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