Benzeneethanol, beta-methoxy- → 2-Methoxy-2-phenylethanal

HRID 1440875Notes

Reaction equation

HRID 1440875 reaction equation
[C:1]1([CH:7]([O:10][CH2:11]CC)[CH2:8][OH:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.COC(C1C=CC=CC=1)CO>>[C:1]1([CH:7]([O:10][CH3:11])[CH:8]=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 102910Benzeneethanol, beta-methoxy-HCID 109868792-Phenyl-2-propoxyethanol

Product 1

HCID 116439512-Methoxy-2-phenylethanalYield 69.8%

Procedure

The procedure in Example 3 was repeated except that 180.25 g of 2-phenyl-2-propoxyethanol was replaced with 152 g of 2-methoxy-2-phenylethanol, to obtain 104.8 g of 2-phenyl-2-methoxyethanal (yield: 69%).

Sources & evidence

ORD record
ord-35f018865130441f94d67eb4f0ea27f9
Source dataset
uspto-grants-1996_03
Patent number
US05500484

Reaction notes

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