HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl(2-oxo-2-phenylethyl)sulfanium bromide → HCID 19047920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl(2-oxo-2-phenylethyl)sulfanium bromide | HCID 213007 | — |
| Reactant | HCID 23668465 | HCID 23668465 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19047920 | HCID 19047920 | 61.1% |
Reaction Steps
An aqueous solution of 5.424 g of lithium butyltriphenylborate in 100 ml of water was added to an aqueous solution of 5.090 g of dimethylphenacylsulfonium bromide in 200 ml of water, and the resultant mixture was stirred at room temperature for 30 minutes. The reaction mixture was filtered, and the resultant crystal was washed with water and dried to give 5.202 g of dimethylphenacylsulfonium-butyltriphenylborate as a white crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05500453 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-2bc82f63e82b478984cf9c2e224b354d |
| Source note | uspto-grants-1996_03 |