HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23284049, compound → HCID 18982357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23284049 | HCID 23284049 | — |
| Reactant | HCID 23668465 | HCID 23668465 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18982357 | HCID 18982357 | 84.8% |
Reaction Steps
An aqueous solution of 4.98 g of lithium butyltriphenylborate in 100 ml of water was added to an aqueous solution of 4.20 g of dimethyl-p-cyanobenzylsulfonium bromide in 100 ml of water, and the resultant mixture was stirred at room temperature for 30 minutes. Then, the reaction mixture was filtered, and the resultant crystal was washed with water and dried to give 6.59 g of dimethyl-p-cyanobenzylsulfonium-butyltriphenylborate as a white crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05500453 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-545364e9a7754bfc994ba79041aad984 |
| Source note | uspto-grants-1996_03 |