HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl(2-oxo-2-phenylethyl)sulfanium bromide → HCID 18982280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl(2-oxo-2-phenylethyl)sulfanium bromide | HCID 213007 | — |
| Reactant | HCID 131719320 | HCID 131719320 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18982280 | HCID 18982280 | 82.2% |
Reaction Steps
An aqueous solution of 6.51 g of lithium benzyltriphenylborate in 100 ml of water was added to an aqueous solution of 5.00 g of dimethylphenacylsulfonium bromide in 200 ml of water, and the resultant mixture was stirred at room temperature for 30 minutes. Then, the reaction mixture was filtered, and the resultant crystal was washed with water and dried to give 8.09 g of dimethylphenacylsulfonium-benzyltriphenylborate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05500453 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-f7e420c7756c4293be466bc1a90db18b |
| Source note | uspto-grants-1996_03 |