HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl(2-oxo-2-phenylethyl)sulfanium bromide → HCID 18982323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl(2-oxo-2-phenylethyl)sulfanium bromide | HCID 213007 | — |
| Reactant | HCID 131719321 | HCID 131719321 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18982323 | HCID 18982323 | 78.1% |
Reaction Steps
An aqueous solution of 2.11 g of lithium vinyltriphenylborate in 100 ml of water was added to an aqueous solution of 2.00 g of dimethylphenacylsulfonium bromide in 50 ml of water, and the resultant mixture was stirred at room temperature for 30 minutes. Then, the reaction mixture was filtered, and the resultant crystal was washed with water and dried to give 2.69 g of dimethylphenacylsulfonium-vinyltriphenylborate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05500453 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-78468bf380a6418a8f21b47dc458079e |
| Source note | uspto-grants-1996_03 |