HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl(2-oxo-2-phenylethyl)sulfanium bromide → HCID 18982245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl(2-oxo-2-phenylethyl)sulfanium bromide | HCID 213007 | — |
| Reactant | HCID 88360627 | HCID 88360627 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18982245 | HCID 18982245 | 70.9% |
Reaction Steps
An aqueous solution of 2.76 g of lithium butyltris(p-fluorophenyl)borate in 100 ml of water was added to an aqueous solution of 2.00 g of dimethylphenacylsulfonium bromide in 50 ml of water, and the resultant mixture was stirred at room temperature for 30 minutes. Then, the reaction mixture was filtered, and the resultant crystal was washed with water and dried to give 2.90 g of dimethylphenacylsulfonium-butyltris(p-fluorophenyl)borate as a white crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05500453 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-cc4d0f2176054ee2bf00c662dfffc9b3 |
| Source note | uspto-grants-1996_03 |