HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Ethoxy-2-oxoethyl)dimethylsulphonium bromide → HCID 18982304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Ethoxy-2-oxoethyl)dimethylsulphonium bromide | HCID 78861 | — |
| Reactant | HCID 23668465 | HCID 23668465 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18982304 | HCID 18982304 | 86.3% |
Reaction Steps
An aqueous solution of 5.00 g of lithium butyltriphenylborate in 100 ml of water was added to an aqueous solution of 3.74 g of dimethylethoxycarbonylmethylsulfonium bromide in 200 ml of water, and the resultant mixture was stirred at room temperature for 30 minutes. Then, the reaction mixture was filtered, and the resultant crystal was washed with water and dried to give 6.32 g of dimethylethoxycarbonylmethylsulfonium-butyltriphenylborate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05500453 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-72e6abe30e3f4f84bb3faf0a30a9b3ec |
| Source note | uspto-grants-1996_03 |