Water → HCID 18982537, compound

Participants

Reaction Steps

A solution of 3.00 g of lithium butyltriphenylborate in 100 ml of acetonitrile was added to a solution of 2.75 g of di-tert-butyl-N-cyclohexylaminosulfonium chloride in 100 ml of methanol, and the resultant mixture was stirred at room temperature for 30 minutes. The reaction mixture was poured into 500 ml of water, and the resultant oily component was separated, recovered, washed with water and recrystallized from dichloromethane/ether to give 2.52 g of di-tert-butyl-N-cyclohexylaminosulfonium-butyltriphenylborate.

Provenance & Evidence