Water → HCID 18982532, compound

Participants

Reaction Steps

A solution of 2.62 g of lithium methyl-tris(p-fluorophenyl)borate in 50 ml of acetonitrile was added to a solution of 5.00 g of bis(p-chlorophenyl)(p-methoxyphenacyl)oxosulfoniumhexafluorophosphate in 100 ml of acetonitrile, and the resultant mixture was stirred at room temperature for 30 minutes. Then, 200 ml of water was added. The resultant precipitate of a yellow oily component was recovered, and 100 ml of dichloromethane was added. The dichloromethane layer was washed with water, dried and concentrated to give 3.26 g of bis(p-chlorophenyl)(p-methoxyphenacyl)oxosulfonium-methyl-tris(p-fluorophenyl)borate.

Provenance & Evidence