Water → HCID 18982288, compound

Participants

Reaction Steps

A solution of 1.69 g of lithium tert-butyltriethylborate in 50 ml of acetonitrile was added to solution of 5.00 g of diphenyl(p-methylbenzyl)sulfonium hexafluoroarsenate in 100 ml of acetonitrile, and the resultant mixture was stirred at room temperature for 30 minutes. Then, 200 ml of water was added. The resultant precipitate of a yellow oily component was recovered, and 100 ml of dichloromethane was added. The dichloromethane layer was washed with water, dried and concentrated to give 1.28 g of diphenyl(p-methylbenzyl)sulfonium-(tert-butyl)triethylborate.

Provenance & Evidence