Water → HCID 131719337, compound

Participants

Reaction Steps

A solution of 3.48 g of lithium (2-phenylethenyl)tris(p-fluorophenyl)borate in 50 ml of acetonitrile was added to a solution of 5.00 g of bis(p-chlorophenyl)(p-bromobenzyl)oxosulfonium hexafluorophosphatc in 100 ml of acetonitrile, and the resultant mixture was stirred at room temperature for 30 minutes. Then, 200 ml of water was added. The resultant precipitate of a yellow oily component was recovered, and 100 ml of dichloromethane was added. The dichloromethane layer was washed with water, dried and concentrated to give 1.95 g of (p-chlorophenyl)(p-bromobenzyl)oxosulfonium(2-phenylethenyl)tris(p-fluorophenyl)borate.

Provenance & Evidence