Water → HCID 131719340, compound

Participants

Reaction Steps

A solution of 4.17 g of lithium tetramethylammonium methyltris(p-methoxyphenyl)borate in 50 ml of acetonitrile was added to a solution of 5.00 g of bis(p-chlorophenyl)(3,3-dicyano-2-methyl-2-propenyl)sulfonium hexafluorophosphate in 100 ml of acetonitrile, and the resultant mixture was stirred at room temperature for 30 minutes. Then, 200 ml of water was added. The resultant precipitate of a yellow oily component was recovered, and 100 ml of dichloromethane was added. The dichloromethane layer was washed with water, dried and concentrated to give 2.85 g of bis(p-chlorophenyl)(3,3-dicyano-2-methyl-2-propenyl) sulfonium-methyltris(p-methoxyphenyl)borate.

Provenance & Evidence