HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 15332560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 15332559 | HCID 15332559 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15332560 | HCID 15332560 | — |
Reaction Steps
By the method of Example 1, Step B, 9.79 g (0.042 mole) of 4-(2,4-dichlorophenyl)butanoic acid and 5.8 g (0.050 mole) of oxalyl chloride are reacted in 75 mL of diethyl ether and two drops of N,N-dimethylformamide, yielding 4-(2,4-dichlorophenyl)butanoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05502054 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-4c1fd7f5f56f460a91ece53c37634d01 |
| Source note | uspto-grants-1996_03 |