HCID 68686878, compound → HCID 68687072, compound

HRID 1441369Notes

Reaction equation

HRID 1441369 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([N:10]2[CH2:14][CH2:13][C@H:12]([NH:15][C:16](=[O:18])[CH3:17])[CH2:11]2)=[CH:6][CH:5]=1)([O-])=O>CCO>[NH2:1][C:4]1[CH:5]=[CH:6][C:7]([N:10]2[CH2:14][CH2:13][C@H:12]([NH:15][C:16](=[O:18])[CH3:17])[CH2:11]2)=[CH:8][CH:9]=1

Participants

3

Reactant 1

HCID 68686878HCID 68686878, compound

Product 1

HCID 68687072HCID 68687072, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The title compound was prepared by the procedure of Method 43 starting from N-[(3S)-1-(4-nitrophenyl)pyrrolidin-3-yl]acetamide (Method 48). NMR: 1.79 (s, 3H), 1.69-1.88 (m, 1H), 2.07-2.20 (m, 1H), 2.82-2.93 (m, 1H), 3.01-3.14 (m, 1H), 3.16-3.38 (m, 2H), 4.25-4.36 (m, 1H), 6.31 (d, 2H), 6.51 (d, 2H), 8.08 (d, 1H)+EtOH.

Sources & evidence

ORD record
ord-ac62f973ddf040d2aff585d476341d4d
Source dataset
uspto-grants-2010_02
Patent number
US07655652B2

Reaction notes

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