HuagongsheHuagongshe Chemistry Print Report · For research reference only
2(3H)-Benzothiazolone, 6-nitro- → 2(3H)-Benzothiazolone, 6-amino-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2(3H)-Benzothiazolone, 6-nitro- | HCID 641571 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2(3H)-Benzothiazolone, 6-amino- | HCID 6453329 | 96.3% |
Reaction Steps
A solution of 6-nitro-2-benzothiazolinone (98 mg, 0.50 mmol) in 20 ml of EtOAc with 10% Pd/C (˜20 mg) was stirred under H2 balloon for 4 h. The reaction mixture was filtered through celite eluting with EtOAc, concentrated under reduced pressure to give 80 mg of 6-amino-2-benzothiazolinone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07655688B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-31c2ebe59f674e9cb56caa0268e5f911 |
| Source note | uspto-grants-2010_02 |