Pyridine → HCID 11587138, compound

Participants

Reaction Steps

Mixture of quinolin-6-ol (0.58 g., 4 mmol), hexyl isocyanate (0.698 ml, 4.8 mmol) and of dry pyridine (0.3 ml) in dry dioxane (10 ml) was heated at 100° C. with stirring for 3 hours. Reaction mixture was concentrated under vaccum, the residue was titurated with water (1 ml) and crystallised with ether to give 1a; yield: 0.75 g. (68.93%).

Provenance & Evidence