HCID 59165785, compound → HCID 58864521, compound

Participants

Reaction Steps

10% Palladium on carbon (200 mg) was added to a solution of 1-tert-butyl 4-ethyl 4-(5-chloro-2-nitrobenzyl)piperidine-1,4-dicarboxylate (250 mg, 0.586 mmol) in EtOH (15 mL). The reaction vessel was evacuated and back-filled with nitrogen (3×), then back-filled with hydrogen (55 psi). After 24 h, the mixture was filtered though celite and concentrated to give the title compound (0.20 g). MS: m/z=363.1 (M+1).

Provenance & Evidence