Cyclopropanesulfonamide → HCID 76593231, compound

Participants

Reaction Steps

Reaction of the acid 169 with cyclopropane sulfonic acid amide according to the procedure described in example 159, followed by purification on HPLC using an Ace-5 C8 column (100×21.2 mm) and an ammonium acetate buffer 5 mM, pH 6.8, 5% acetonitrile, going from 35 to 60% acetonitrile, gave the title compound as a white solid (8 mg, 7%). LRMS (M+H) 738.

Provenance & Evidence