HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 76593238, compound → HCID 75290665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 76593238 | HCID 76593238 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 75290665 | HCID 75290665 | 64% |
Reaction Steps
Compound 173 (150 mg, 0.18 mmol) was stirred for 30 min in a mixture of dichloromethane-trifluoroacetic acid; 2:1. Evaporation and purification by column chromatography (5% methanol in ether) gave the title compound (81 mg, 62%). MS (M−H)+ 703
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07659245B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-5f2e4e0350b5417b86dd3b86379df42f |
| Source note | uspto-grants-2010_02 |