HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68558866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 66887048 | HCID 66887048 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68558866 | HCID 68558866 | — |
Reaction Steps
To a solution of [1-(1-Benzyl-5-bromo-1H-benzimidazol-2-yl)-2-methyl-propyl]-carbamic acid tert-butyl ester in DCM (2 ml), was added trifluoroacetic acid (0.5 ml). The reaction mixture was stirred at room temperature for 30 minutes. The solvent was removed in vacuo to give the free amine product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662581B1 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-b6dc2d9765dd49028e573b95eaceccf6 |
| Source note | uspto-grants-2010_02 |