4-Fluorobenzoyl chloride → HCID 68565603, compound
Reaction equation
[N:1]12[CH2:9][CH2:8][CH:5]([CH2:6][CH2:7]1)[N:4]([C:10]1[CH:15]=[CH:14][C:13]([NH2:16])=[CH:12][CH:11]=1)[CH2:3][CH2:2]2.[F:17][C:18]1[CH:26]=[CH:25][C:21]([C:22]([Cl:24])=[O:23])=[CH:20][CH:19]=1>>[ClH:24].[N:1]12[CH2:9][CH2:8][CH:5]([CH2:6][CH2:7]1)[N:4]([C:10]1[CH:15]=[CH:14][C:13]([NH:16][C:22](=[O:23])[C:21]3[CH:25]=[CH:26][C:18]([F:17])=[CH:19][CH:20]=3)=[CH:12][CH:11]=1)[CH2:3][CH2:2]2Participants
3
Procedure
Was prepared by Method G from 4-(1,4-diaza-bicyclo[3.2.2]non-4-yl)-phenylamine and 4-fluorobenzoyl chloride. Mp. >270° C. (decomp.).
Sources & evidence
- ORD record
- ord-2b83e1e763f84b70a1da95052be58185
- Source dataset
- uspto-grants-2010_02
- Patent number
- US07662808B2
Reaction notes
Loading…