4-Nitrobenzoyl chloride → HCID 68565947, compound

HRID 1443779Notes

Reaction equation

HRID 1443779 reaction equation
[N:1]12[CH2:9][CH2:8][CH:5]([CH2:6][CH2:7]1)[N:4]([C:10]1[N:15]=[CH:14][C:13]([NH2:16])=[CH:12][CH:11]=1)[CH2:3][CH2:2]2.[N+:17]([C:20]1[CH:28]=[CH:27][C:23]([C:24]([Cl:26])=[O:25])=[CH:22][CH:21]=1)([O-:19])=[O:18]>>[ClH:26].[N:1]12[CH2:7][CH2:6][CH:5]([CH2:8][CH2:9]1)[N:4]([C:10]1[N:15]=[CH:14][C:13]([NH:16][C:24](=[O:25])[C:23]3[CH:22]=[CH:21][C:20]([N+:17]([O-:19])=[O:18])=[CH:28][CH:27]=3)=[CH:12][CH:11]=1)[CH2:3][CH2:2]2

Participants

3

Reactant 2

HCID 85024-Nitrobenzoyl chlorideHCID 68565532HCID 68565532, compound

Product 1

HCID 68565947HCID 68565947, compound

Procedure

Was prepared according to Method G from 6-(1,4-diaza-bicyclo[3.2.2]non-4-yl)-pyridin-3-ylamine and 4-nitrobenzoyl chloride. Mp. >310° C. (decomp.).

Workup

  1. customWas prepared

Sources & evidence

ORD record
ord-99c1476bcff14e5e93c1dfe9c8d84afd
Source dataset
uspto-grants-2010_02
Patent number
US07662808B2

Reaction notes

Loading…