3-(Trifluoromethyl)phenyl isocyanate → HCID 86620419, compound

HRID 1443809Notes

Reaction equation

HRID 1443809 reaction equation
C1(P(=[N:20][C:21]2[CH:26]=[CH:25][N:24]=[CH:23][C:22]=2/[CH:27]=[CH:28]/[C:29]([O:31][CH3:32])=[O:30])(C2C=CC=CC=2)C2C=CC=CC=2)C=CC=CC=1.[F:33][C:34]([F:45])([F:44])[C:35]1[CH:36]=[C:37]([N:41]=[C:42]=O)[CH:38]=[CH:39][CH:40]=1>>[F:33][C:34]([F:44])([F:45])[C:35]1[CH:36]=[C:37]([N:41]=[C:42]=[N:20][C:21]2[CH:26]=[CH:25][N:24]=[CH:23][C:22]=2/[CH:27]=[CH:28]/[C:29]([O:31][CH3:32])=[O:30])[CH:38]=[CH:39][CH:40]=1

Participants

3

Reactant 2

HCID 94833-(Trifluoromethyl)phenyl isocyanateHCID 59168062HCID 59168062, compound

Product 1

HCID 86620419HCID 86620419, compound

Procedure

300 mg (0.34 mmol) of iminophosphorane from Example 12A are reacted by general procedure [B] with 70 mg (0.38 mmol) of 3-trifluoromethylphenyl isocyanate, and the crude product is reacted further without purification.

Sources & evidence

ORD record
ord-682a7f3c9536492f94c311448738d528
Source dataset
uspto-grants-2010_02
Patent number
US07662822B2

Reaction notes

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