Potassium Nitrate → HCID 59168385, compound

HRID 1443910Notes

Reaction equation

HRID 1443910 reaction equation
[CH:1]1[CH:9]=[CH:8][C:7]2[CH2:10][CH2:11][N:5]3[C:6]=2[C:2]=1[C:3]1[CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][C:4]=13.[N+:17]([O-])([O-:19])=[O:18].[K+]>S(=O)(=O)(O)O>[N+:17]([C:9]1[CH:1]=[C:2]2[C:6]3=[C:7]([CH2:10][CH2:11][N:5]3[C:4]3[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:3]2=3)[CH:8]=1)([O-:19])=[O:18]

Participants

4

Reactant 2

HCID 24434Potassium NitrateHCID 13464802HCID 13464802, compound

Product 1

HCID 59168385HCID 59168385, compound

Reagents, catalysts & solvents 1

HCID 1118Sulfuric AcidSolvent

Procedure

Following the procedure of Example 1, step 2, 4,5,8,9,10,11-hexahydro-7H-cyclohepta[b]pyrrolo[3,2,1-hi]indole (7.5 g, 35 mmol) and potassium nitrate (3.6 g, 35 mmol) in concentrated sulfuric acid (100 mL) provided 2-nitro-4,5,8,9,10,11-hexahydro-7H-cyclohepta[b]pyrrolo[3,2,1-hi]indole.

Sources & evidence

ORD record
ord-5dec50b8b23b4d7283d9df32586a21d5
Source dataset
uspto-grants-2010_02
Patent number
US07662831B2

Reaction notes

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